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Table 3 Contents of the main bioactive compounds identified in the Mix1 analyzed in negative-ionization mode

From: Natural chemotherapeutic alternatives for controlling of haemonchosis in sheep

No. Compound RT (min) UV m/z [M-H] Formula MS2 main ion MS2 fragments mg/g DM
1 4-O-Caffeoylquinic acid 3.8 215/325 353.0880 C16H18O9 191.0553   0.71
2 3-O-Caffeoylquinic acid 5.2 215/325 353.0880 C16H18O9 191.0556 179/161/135 11.3
3 5-O-Caffeoylquinic acid 5.5 215/325 353.0880 C16H18O9 191.0557   0.73
4 Caffeic acid 6.9 215/324 179.0339 C9H8O4 135.0435   0.81
5 1-O-Feruloylglucose 8.0 215/324 355.1041 C16H20O9 193.0498 149/0589/134 0.38
6 3-O-p-Coumaroylquinic acid 8.7 215/325 337.0933 C16H18O8 191.0187 173 0.65
7 4-O-p-Coumaroylquinic acid 9.5 215/325 337.0933 C16H18O8 191.0187 173 3.45
8 Caffeoylmalic acid 9.7 313/000 295.0455 C13H12O8 179.0336 133/207 1.42
9 4-Caffeoylshikimic acid 11.1 215/325 335.0768 C16H16O8 179.0334 161/191/135 6.40
10 Glucodistylin 11.5 218/295 465.1024 C21H22O12 285.0405 303/177 4.90
11 Myricetin 3-O-galactosid 12.2 271/345 479.0828 C21H20O13 317.0297   20.2
12 Quercetin O-Pen-Hex 12.3 252/351 595.1298 C26H28O16 300.0273   2.63
13 Quercetin O-Hex-O-Dhex 12.4 252/351 609.1442 C27H30O16 447.1131 152/429/161/179 0.96
14 Luteolin O-diglucuronide 12.5 255/340 637.1029 C27H26O18 461.0707 285/04 0.26
15 Rutin 13.5 255/342 609.1451 C27H30O16 300.0275   2.96
16 Acetoside (verbascoside) 13.9 218/291/331 623.1972 C29H36O15 461.1657 161/153/179/135 0.63
17 Quercetin O-Hex 15.0 257/351 463.0874 C21H20O12 300.0273   0.02
18 Quercetagetin 3′-methyl-ether 7-glucoside 15.1 252/351 493.0977 C22H22O13 447.0928 331/285 0.30
19 3,5-Dicaffeoylquinic acid 15.2 215/325 515.1195 C25H24O12 353.0877 173/179/335/191/161 0.42
20 Quercetin O-Pen 15.3 252/351 433.0776 C20H18O11 300.0277 271/255/151 1.41
21 1,5-Dicaffeoylquinic acid 15.4 215/325 515.1194 C25H24O12 353.0885 191/179/135 15.4
22 Qquercitrin 15.4 256/348 447.0904 C21H20O11 300.0276   1.88
23 Apigenin O-Hex 15.5 267/341 431.0983 C21H20O10 268.0371   0.33
24 Isorhamnetin O-Dhex-Dhex 15.7 267/349 607.1666 C28H32O15 299.058 284 0.15
25 Quercetin O-(Hex-Ac) 15.9 267/340 505.0969 C23H22O13 300.0727   0.24
26 Rosmarinic acid 16.1 218/287/329 359.0781 C18H16O8 161.023 197/179 5.95
27 Kaempferol O-glucuronide 27.2   461.0727 C21H18O12 285.0406 137 0.23
28 3-Dihydrocaffeoyl-4-caffeoyl quinic acid 16.4 215,325 517.1354 C25H26O12 355.1239 161/179/323 9.72
29 Kaempferol O-(Hex-Ac) 16.8   489.1036 C23H22O12 284.0325 255/227/327 0.72
30 Myricitrin glucuronide 18.5   519.1143 C24H24O13 314.0435 269/243/357 0.76
31 Apigenin O-(Hex-Ac) 18.8   473.1093 C23H22O11 268.0378   0.73
32 Biochanin A-hexurunosyl-hexurunosyl 19.5   637.1774 C29H34O16 283.0618   0.65
33 Apigenin O-(Hex-Ac) 20.1   473.1095 C23H22O11 268.0382   1.57