Skip to main content

Table 1 13C NMR (100 MHz) data of Compounds 1 − 2a

From: Determine the structure of phosphorylated modification of icariin and its antiviral activity against duck hepatitis virus A

 

1 b

2 b

position

δC,type

δC,type

2

157.80,C

157.79,C

3

135.11,C

135.12,C

4

178.77,C

178.77,C

5

160.98,C

160.99,C

6

98.59,CH

98.60,CH

7

161.88,C

161.89,C

8

108.77,C

108.78,C

9

153.48,C

153.49,C

10

106.06,C

106.07,C

11

21.89,CH2

21.90,CH2

12

122.60,CH

122.61,CH

13

131.58,C

131.58,C

14

25.94,CH3

25.93,CH3

15

18.33,CH3

18.33,CH3

1'

122.73,C

122.74,C

2',6'

131.04,CH

131.04,CH

3',5'

114.55,CH

114.56,CH

4'

159.56,C

159.56,C

1''

102.46,CH

102.46,CH

2''

70.12,CH

70.13,CH

3''

70.55,CH

70.55,CH

4''

71.18,CH

71.17,CH

5''

70.78,CH

70.79,CH

6''

17.93,CH3

17.93,CH3

1'''

101.01,CH

101.01,CH

2'''

73.83,CH

73.84,CH

3'''

77.07,CH

77.08,CH

4'''

71.58,CH

71.85,CH

5'''

77.66,CH

77.67,CH

6'''

61.10,CH2

70.17,CH2

OCH3

55.98,CH3

55.99,CH3

  1. aThe chemical shifts (δ) are expressed in parts per million. bData recorded in dimethyl sulfoxide-d6