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Table 4 Contents of the main bioactive compounds identified in the Mix2 analyzed in negative-ionization mode

From: Natural chemotherapeutic alternatives for controlling of haemonchosis in sheep

No.

Compound

RT (min)

UV

m/z [M-H]

Formula

MS2 main ion

MS2 fragments

mg/g DM

1

3-O-Caffeoylquinic acid

4.7

215/325

353.0880

C16H18O9

191.0553

179/161/135

6.91

2

2-O-Caffeoylhydroxycitric acid

5.2

215/324

369.0464

C15H14O11

189.003

127/207/179

0.78

3

1-O-Feruloylglucose

5.7

215/324

355.1046

C16H20O9

193.0498

149/0589/134

0.50

4

Caffeic acid

6.1

 

179.0342

C9H8O4

135.0436

 

1.09

5

Caffeoylmalic acid

6.2

250/324

295.046

C13H12O8

179.0336

133/207

1.27

6

2-O-Feruloylhydroxycitric acid

8.2

215/324

383.0623

C16H16O11

189.0039

191/337/127

3.64

7

N-Malonyl-D-phenylalanine

8.3

 

250.0723

C12H13NO5

165.055

207

1.88

8

Astilbin

9.2

 

449.1089

C21H22O11

287.0561

259/243

1.07

9

Nigellicine

9.4

 

245.0934

C13H14N2O3

203.0829

 

0.69

10

Quercetin O-Pen-Hex

10.1

255/352

595.1298

C26H28O16

300.0273

 

0.48

11

Isoquercitrin O-Dhex

10.2

252/351

609.1459

C27H30O16

300.0279

 

0.54

12

Quercetin O-Hex

10.5

252/351

463.0874

C21H20O12

301.0366

141/151

2.25

13

Typhaneoside

10.8

255/354

769.2207

C34H42O20

314.0436

595

2.71

14

Rutin

11.0

255/352

609.1451

C27H30O16

300.0275

 

5.73

15

6-Hydroxykaempferol 7-glucoside isoquercitrin

11.5

264/341

463.089

C21H20O12

300.0284

 

1.64

16

Quercetin-O-glucuronide

12.2

255/352

477.0681

C21H18O13

301.0359

 

0.85

17

Kaempferol O-Hex

12.3

265/343

447.0937

C21H20O11

285.0407

 

1.0

18

Sorhamnetin 3-O-Dhex-Hex

12.9

 

623.1631

C28H33O16

314.0436

461/161

0.25

19

Patuletin O-Hex

13.0

256/351

493.099

C22H22O13

331.0469

447/285/151

0.41

20

3,5-Dicaffeoylquinic acid

13.2

215/325

515.1208

C25H24O12

353.0885

173/179/191

0.92

21

Luteolin-O-Hex-Dhex

13.9

265/343

593.1518

C27H30O15

285.0409

 

1.43

22

Calendoflavoside

14.1

351/000

623.1627

C28H33O16

315.0515

269

0.71

23

3,4-Dicaffeoylquinic acid

14.5

215/326

515.1208

C25H24O12

353.0885

173/179/191

0.44

24

Apigenin O-Hex

14.7

266/339

431.0994

C21H20O10

268.0382

 

2.82

25

Isorhamnetin-O-Hex

14.9

267/338

447.0928

C21H20O11

284.0332

300/0279/327/255

1.11

26

1,5-Dicaffeoylquinic acid

15.2

214/325

515.1206

C25H24O12

353.0885

173/179/191

6.18

27

Isorhamnetin O-(Hex-Ac)

15.3

260/000

519.1141

C24H24O13

314.0436

331/299

1.75

28

Quercetin O-(Hex-Ac)

15.4

255/355

505.0963

C23H22O13

300.0275

271

0.25

29

3-caffeoyl-4-dihydrocaffeoyl quinic acid

15.9

215/325

517.1358

C25H26O12

323.0779

193/161/179/149/221

0.49

30

Apigenin O-(Hex-Ac)

16.5

265/325

473.1101

C23H22O11

268.0385

 

1.94